Synonyms
(±)-1,2-dithiolane-3-pentanoic acid, 6,8-dithiooctanoic acid, dl-α-lipoic acid, dl-6,8-thioctic acid, lip(s2)
Technical Data
CAS Number: 1077-28-7
Molecular Formula: C8H14O2S2
Molecular Weight: 206.33
Beilstein Registry Number: 81853
EC Number: 214-071-2
FabriChem Specifications
ITEMS | SPECIFICATIONS |
---|---|
Appearance | Yellow crystalline powder |
Identification A. HPLC B. Infrared Absorption | Positive Positive |
Melting Point | 60 – 62°C |
Solubility (1N NaOH) | Clear & Pale Yellow |
Residue on Ignition | 0.10% Max. |
Heavy Metals | 10 ppm Max. |
Chloride | 0.07% Max. |
Loss on Drying (Vacuum 40°C 3hr) | 0.20% Max. |
Assay (by HPLC, USP Method) | 99.0% - 101.0% |
Specific Optical Rotation | 1° to +1° |
Chromatographic Purity (Test 1) A. Individual Impurity B. Total Impurities | A. 0.1% Max. B. 2.0% Max. |
Chromatographic Purity (Test 2) | 2.0% Max. |
Residual Solvents (by GC): | |
Toluene | 30 ppm Max. |
Ethyl Acetate | 0.20% Max. |
Cyclohexane | 0.20% Max. |
Microbiology: | |
Total Aerobic Count | 1,000 CFU/g Max. |
Yeast & Mold | 100 CFU/g Max. |
E. Coli | Not Detectable |
Salmonella | Not Detectable |